#------------------------------------------------------------------------------
#$Date: 2018-09-08 05:01:15 +0300 (Sat, 08 Sep 2018) $
#$Revision: 210555 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/24/26/2242624.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2242624
_cell_angle_alpha                105.224
_cell_angle_beta                 110.601
_cell_angle_gamma                91.389
_cell_length_a                   2.4473
_cell_length_b                   3.4688
_cell_length_c                   3.5144
_exptl_crystal_F_000             54.00
_reflns_d_resolution_high        0.5546
_cod_data_source_file            wm5459Isup2.hkl
_cod_data_source_block           I
_shelx_title                     ' FeN2_s5_1'
_shelx_refln_list_code           4
_shelx_f_calc_maximum            20.06
_shelx_f_squared_multiplier      1.000
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, -z'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
1 1 0 188.70 173.17 0.67 o
2 1 0 241.36 246.01 1.45 o
3 1 0 10.68 11.61 2.79 o
2 2 0 14.15 18.55 1.99 o
3 2 0 50.55 50.77 2.10 o
2 3 0 50.13 62.96 2.28 o
-2 -3 1 113.75 122.59 1.48 o
-3 -2 1 83.55 78.29 1.91 o
-3 -1 1 83.70 85.48 2.08 o
-2 -1 1 37.83 40.49 1.17 o
0 -1 1 303.00 307.70 0.68 o
0 0 1 311.47 316.19 0.63 o
1 0 1 269.00 269.24 1.13 o
2 0 1 120.53 112.06 1.95 o
3 0 1 24.93 22.85 3.56 o
1 1 1 143.07 137.82 1.25 o
2 1 1 72.48 77.88 3.33 o
3 1 1 22.44 26.63 2.78 o
2 2 1 52.89 63.63 2.80 o
3 2 1 37.84 36.43 2.55 o
-1 -2 2 230.30 240.54 1.52 o
0 -2 2 279.02 255.56 1.38 o
-1 -1 2 391.19 371.61 1.28 o
0 -1 2 41.46 32.65 1.10 o
1 -1 2 323.53 319.92 1.80 o
2 -1 2 41.83 43.98 3.46 o
3 -1 2 12.32 9.58 3.79 o
0 0 2 402.59 411.86 1.33 o
1 0 2 147.77 145.83 1.75 o
2 0 2 13.43 11.71 2.08 o
3 0 2 81.00 66.14 3.06 o
1 1 2 22.25 24.04 1.76 o
2 1 2 125.95 137.76 2.31 o
3 1 2 8.53 8.16 3.32 o
2 2 2 27.36 31.77 3.57 o
-1 -3 3 150.44 164.88 2.38 o
0 -3 3 20.81 23.16 2.68 o
-3 -2 3 28.23 26.81 1.42 o
-2 -2 3 196.66 208.31 1.74 o
-1 -2 3 15.71 18.17 1.45 o
0 -2 3 201.63 196.16 1.83 o
1 -2 3 69.38 69.93 2.35 o
-1 -1 3 210.01 209.68 1.55 o
0 -1 3 183.80 186.60 1.83 o
1 -1 3 25.33 24.85 4.30 o
2 -1 3 64.16 59.54 4.00 o
0 0 3 16.78 17.51 4.05 o
1 0 3 137.15 145.48 2.36 o
2 0 3 27.70 22.66 2.55 o
1 1 3 59.11 62.11 3.30 o
2 1 3 11.70 10.21 3.07 o
-1 -4 4 48.82 45.50 3.30 o
-2 -3 4 30.36 21.01 1.84 o
-1 -3 4 52.59 57.15 2.04 o
0 -3 4 43.67 42.39 2.67 o
-2 -2 4 58.33 61.14 2.44 o
-1 -2 4 72.69 80.80 1.99 o
0 -2 4 80.60 86.44 4.83 o
1 -2 4 17.27 10.03 2.52 o
-1 -1 4 57.34 64.42 2.64 o
0 -1 4 55.46 51.08 2.33 o
1 -1 4 40.26 29.52 2.55 o
0 0 4 55.86 60.95 4.90 o
-1 -5 5 6.82 3.81 4.21 o
-2 -4 5 18.26 15.13 3.80 o
-1 -4 5 11.02 10.63 4.93 o
-2 -3 5 8.97 9.26 2.27 o
-1 -3 5 100.58 91.45 3.63 o
-2 -2 5 81.69 84.99 3.30 o
-1 -2 5 19.53 46.98 20.80 o
-2 -3 6 15.64 16.99 3.95 o